文章基本信息

标题：New Compound with Potential Liquid Crystal Properties. III. Synthesis, Characterization and Mesomorphic ordering of N,n’-bis-[4-(4’-octyloxy-benzoic)-ester-benzyliden-n-propyl]-piperazine
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作者：Liliana Cseh ; C. Csunderlik ; Otilia Costisor 等
期刊名称：Universitatea Politehnica din Timisoara. Buletinul Stiintific. Seria Chimie si Ingineria Mediului
印刷版ISSN：1224-6018
出版年度：2005
卷号：50(64)
期号：01-02
出版社：Universitatea Politehnica din Timisoara
摘要：The synthesis of Schiff base - N,N’-bis-[4-(4’-octyloxy-benzoic)-ester-benzyliden-n-propyl]-piperazine (4) in a multistep process is repported. The last step involves the condensation of 4-octyloxy-benzoic acid 4-formyl-phenyl ester aldehyde (3) with 1,4- bis(3-aminopropyl)piperazine. The intermediates as well as the product were characterized by elemental analysis, melting point and IR, ¹H and ¹³C-NMR spectroscopies. The potential mesogenic property of (4) has been checked with a polarising microscope equipped with a heating stage.
关键词：Schiff base, liquid crystals, spectral properties